HomeCompanyProductsApplicationsScale-upContact usNewsEvents

Applications

To download technical notes for the experiments in the table below, register and/or login for access.

Mixing
Liquid homogeneous Equivalent to static mixer at 4 m/s
L/L Equivalent to ½ litre batch at 400 rpm  
G/L > 1 l batch at 600 rpm
G/L/S 5 times better than 100 ml batch
see publication (3)
Liquid homogenous Higher yield than 1 litre batch see publication (4)
Heat transfer
Liquid homogenous reaction time 8 times faster than 1 litre batch
L/S Suzuki reaction
10 times faster than 1 litre batch
 
Solids
Solid formation semicarbazone
Solids formation Nanoparticle clusters  
Slurry Enzyme free on whole cells
Solids formation Grignard reaction  
Solid formation NaCl up to 25%  
Slurry PVA particles, 50-200 micron, up to 30% video
Slurry Alumina particle, 50-200 micron, up to 10%  
Slurry Caesium Carbonate
20-70 micron, up to 10%
Slurry Sodium carbonate in DMF  
Slurry N-iodomorpholinium hydroiodide salt see publication (1)

 

List of reactions:    
Biocatalytic oxidase    
Hoffman reaction    
Suzuki reaction    
Bourne reaction    
Nitration    
Polymerizations    
Grignard reactions    
De-hydrogenations    
Reaction using BuLi    
Heterogeneous catalysis    
Oxidation Reaction    
Counter current extractions  


List of Publications:

1.   Browne, D.L., et al.,  Continuous Flow Processing of Slurries: Evaluation of an Agitated Cell Reactor, Organic Process Research and Development, In Press

2.    Ashe.R, 2010, Shaken not stirred, tce magazine July-August, 39-41

3.    Gómez-Quero, S., et. al., 2011, Liquid phase catalytic hydrodechlorination of 2, 4-dichlorophenol over Pd/Al2O3: Batch vs. continuous operation, Chemical Engineering Journal, vol 166, issue 3, 1044-1051

4.    Delogu, P., Gasparini, G.,  2010, Scale up of Continuous Processes using multistage CSTR’s, Speciality Chemicals Magazine May, 34-35

5.    Gasparini, G., Patel, M., 2009, Flow Reactors and Dynamic Mixing, Speciality Chemicals Magazine April, 22-23

6.    Ashe, R., 2008, Continuous reactors with easy scale-up, Manufacturing Chemist Magazine September, 83-84

7.    Ashe, R., Patel, M., 2008, Marrying efficiency with flexibility, tce magazine July. , 35-37
 

Log on

 
Forgotten password

Not a member yet? Sign up now!






Highlights

Latest Events


Location: Baveno - Lake Maggiore
9th to 11th July 2012

Date: 01/01/0001 00:00:00


Location: Wurzburg, Germany

Date: 14/05/2012 00:00:00